...Graphene & Carbon Nano-Tube...

Dual Quartz Tubes (5"/4") & Three Zones CVD Furnace upto 1200C for Graphene Film - OTF-1200X-III-D5-4

Dual Quartz Tubes (5"/4") & Three Zones CVD Furnace upto 1200C for Graphene Film - OTF-1200X-III-D5-4

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Product Name Dual Quartz Tubes (5"/4") & Three Zones CVD Furnace upto 1200C for Graphene Film - OTF-1200X-III-D5-4
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Product Code OTF-1200X-III-D5-4
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Personalization Upgrade to Eurotherm Temp Programmer (three zone) Upgrade + 15 inch Laptop + USB-to-RS485 Cable

 

OTF-1200X-5-III-D4 is a dual tube and three-zone tube furnace with max. working temperature of 1200°C  for growing thin films on metallic foil by CVD, specially designed for make graphene and the flexible electrode for solar or battery electrode.

SPECIFICATIONS:


Features


  •      •  Dual quartz tube:  130 mm Dia (5"). outside tube suspended by 101 mm Dia (4")  tube inside.
            The metallic foil will be wrapped inside tube surface for CVD reaction
  •      •  Vacuum sealing flanges for the dual tube, which allow reactive gas go through between two tubes
            ( 20mm space ) for reaction, and forced air can go through the central tube for fast cooling.
  •      •  Max. Working Temperature:  1200°C  
  •      •  Valve and vacuum gauge are included
  •      •  Please click picture on the right to see principal of the furnace
         
         Please click below for a related article:  "Roll-to-roll production of 30-inch graphene films for transparent
         electrodes
"



Furnace structure

  •      •  Three heating zones: (900mm, 36" in total)
    •          º  Zone 1: 300mm  (11.8")
    •          º  Zone 2: 300mm  (11.8")
    •          º  Zone 3: 300 mm (11.8")
  •      •  Max. 25" (625 mm) long with +/- 1°C accuracy if set three zones at the same temperature.
  •      •  Three precision temperature controllers with 30 segment  programmable and +/- 1° C accuracy.
  •      •  Max. Working Temperature:  1200°C
  •      •  Continuous Working Temperature:  1100°C
  •      •  Heating Rate: <= 20°C /min  
  •      •  Constant Temperature Zone: 25" (625 mm) length
             (Three zones are heating at equal temperature simultaneously)
  •          

 
Power

  •      •   AC 208-240V Single Phase, 50/60 Hz (40A breaker required).
  •      •  7 KW  Max.
  •      •  Powder cord is included without a plug.
  •      •  CE certified

Processing Tubes

  •      •  Two High purity Fused Quartz Tubes included
  •      •  Outside tube: 130mm O.D. x 122 mm I.D. x 1480 mm
  •      •  Inside tube: 102mm O.D. x   94 mm I.D. x 1800 mm

Vacuum sealed flanges

  •      •  One pair of flange made of SS304, which seals tightly between tubes by two high-temperature
            O-rings (10-2 by the mechanical pump and 10-5 by the molecular pump ).
  •      •  The flange is built with water cooling jacket. When working temperature over 900°C, it is required
             to use cooling water. You may either use tap water or use our chilling water circulation at picture
             below
  •      •  One KF25 adapter is installed on the left flange to connect a vacuum pump.
  •      •  One stainless steel needle valve is installed on right flange (please choose connector at picture
            below before order)
  •      •  Optional.  You may order a  Compact  Liquid Vaporization Systems for better CVD
           ( Click picture below right )
                             


Thermal Block Placement
     
   



 Optional

Copper Foil for Graphene Growth (150m length x 150mm width x 25um thickness) - EQ-bccf-25u

 

 Furnace Dimension1030 x 430 x 580 mm  ( not included flange and tube )
Net Weightabout 90 kg
Shipping package size after crating65"x45"x35"
WarrantyOne year limited warranty for electrical parts. (Consumable parts such as processing tubes, O-rings, and heating elements are not covered by the warranty, please order the replacement at related products below.)

Laptop, software & WiFi Control(Optional)

  •      •  Brand new laptop with Microsoft Window 10 and Microsoft Office 2013 (30 days free trial) for
             immediate use.
  •      •  Labview Based Temperature Control System (EQ-MTS01) enables user to edit temperature
            profile, manage heat-treatment recipe, record and plot data for MTI furnaces.
  •      •  A wireless remote control provides up to 300 meters operating range.
  •      •  Above features are available upon request at an extra cost (up to $1,000). Please contact us for
            more information.
  •      •  Note:
            The software is only compatible with MTI’s Yudian Temperature Controller

                


Compliance

  •      •  CE Certified
  •      •  All electric components ( >24V) are UL / MET / CSA certified
  •      •  The furnace is ready to pass TUV(UL61010) or CSA certification at extra cost.
           ( please click marks below to learn details )

                    


Related instruction video


   


Updated idea

  •      •  You may put the furnace on a 1200 mm length mobile cart ( click picture on left to order )
  •      •  you may order our gas mixing module to support the furnace and deliver multi-gas to the dual
             tube furnace
  •          


Warning

Click here to learn the installation of a gas regulator

  •      •  All quartz tube furnaces  are designed for using under vacuum and low pressure < 0.2 bars / 3 psi /
            0.02 Mpa

  •      •  Attention: A two-stage pressure regulator must be installed on the gas
            cylinder to limit the pressure to below 3 PSI for safe operation.
     
               Click here to learn the installation of a gas regulator.

  •      •  Vacuum limit definition for all quartz tube furnaces: * Vacuum pressures may only be safely
            used up to 1000°C

  •      •  The flow rate for gasses should be limited to<200 SCCM (or 200ml/min) for reducing thermal
             shocks to the tube

  •      •  For the use of flammable gasses such as H2 and CH4, please consult with MTI technical team
             for safety measures. We Strongly suggest that the furnace needs to be operated inside a fume
             hood with H2/CH4 leaking detector installed.


Application Note

  • After CVD, the graphene must be transferred from the metal catalyst to another substrate for most applications. By using
    the graphene transfer tape, the residue can be low.


Optional Vacuum Package
 (Chose high vacuum pump or low vacuum pump upon customer's requirement)

DescriptionQuantitylinksUnit Price

High Vacuum Pump:  Movable Vacuum Pumping Station Combining Rough & Turbo Pump (up to 1E-7 mbar) with Completed Accessories - EQ-PV-HVS3

1USD$16,850.00
Low Vacuum Dry Pump: Pfeiffer's High Speed ( 226L/min) Oilless Dry Vacuum Pump, 10E-3 Torr Limit - EQ-Adixen-ACP151USD$6695.00
Digital Vacuum Gauge Up to 10-4 Torr1USD$465.95
Vacuum bellows with KF-D25 adapter (1m)1USD$199.95
1/4NPS to KF-D25 quick adapter1
USD$49.95
Quick Clamp with Rubber O-Ring for KF-D25 Vacuum adapter2USD$29.95
If PC control required, please order three sets of software and interface device here1USD$219.00